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The results for the catechins are summarized in Table 2. It can be seen from Table 2 that the content of total polyphenols ranged from 7.
Of the selected 20 tea samples, Bi luo chun green tea had the highest content of polyphenols and catechins. In addition, the correlation between catechins and total polyphenols in the 20 samples from the four types of tea was tested.
The results, shown in Figure 3 , reveal a strong positive correlation between catechins and total polyphenols. Table 2 lists the contents of individual catechins in the four types of tea.
It is apparent that the content of esterified catechins EGCG or ECG is higher than that of nonesterified catechins catechin, EC, or EGC. In comparison of the four types of tea, EGCG content was the highest in green tea 5.
With the increase in the degree of fermentation, the EGCG content gradually decreased and the range of EGCG content in dark tea is only 0.
Among the four types of tea, the ECG content was the highest in black tea 3. A straight calibration curve was obtained for trolox antioxidant activity in the concentration range of 1.
Figure 4 shows the ORAC values of the selected tea samples; the ORAC value ranged from Huang shan mao feng green tea showed the strongest antioxidant activity.
Figure 5 shows the relationships between the ORAC value and total polyphenols and catechins, respectively. A positive correlation was observed in each case, with for total polyphenols and for catechins.
In addition, the correlations between individual catechin content and ORAC values in 20 samples were evaluated. The correlations between ORAC value and content of catechin, EGC, EC, EGCG, and ECG, respectively, are shown in Table 3 , which shows a positive correlation for each case.
In green tea, the EC content showed a relatively higher positive correlation with ORAC values than catechin, EGC, EGCG, and ECG, and the values were significantly different.
For black tea, the EGCG content showed a relatively higher positive correlation with ORAC values than catechin, EC, EGC, and ECG, and the values were significantly different.
In contrast, the correlation coefficients between ORAC value and content of individual catechin in oolong tea and in dark tea infusions were not significantly different.
The free radical-scavenging activity of the 20 samples of the four types of tea was assessed by DPPH assay; the results are shown in Figure 6.
All sample extracts showed good inhibitory activity against the DPPH radical in a dose-dependent manner. The EC50 and AE values of the tea sample extracts are summarized in Table 4 , where lower EC50 values or higher AE values suggest higher antioxidant activity.
For the 20 selected tea samples, EC50 was in the range 0. The scavenging efficiency of Huang shan mao feng green tea against the DPPH radical was the strongest; its EC50 and AE values were 0.
Figure 7 shows the respective correlations between the AE values and the content of total catechins and total polyphenols.
In each case, good correlation was observed for total catechins; for total polyphenols. The correlations between AE values and the content of individual catechins in the 20 tea infusions are summarized in Table 5 ; significant positive correlation was observed in each case.
Among the individual catechins in green tea, the EGCG content showed a relatively higher positive correlation with AE values than those of catechin, EC, EGC, and ECG, and the values were significantly different.
In the tests of antioxidant capacity in the 20 samples of tea, as measured by the DPPH method, it was not clear which component played the important role in antioxidant activity.
The recent development of the online HPLC DPPH method was used to our advantage in this study. This method, which is now used widely in the testing of food and agricultural products and in the pharmaceutical industry [ 35 — 37 ], allows the radical-scavenging activity of a single substance to be measured.
Thus, the radical-scavenging activities of the major catechins EGC, EC, EGCG, ECG, and catechin , gallic acid, and caffeine were determined by the online HPLC DPPH screening method.
The chromatograms of the mixed catechin standards and that of a tea sample are shown in Figure 8 , illustrating the excellent baseline separation of EGC, EC, EGCG, ECG, catechin, gallic acid, and caffeine.
The results showed that while caffeine had almost no DPPH-scavenging activity, strong positive correlations were observed for the contents of the respective HPLC-separated catechins and for gallic acid see Figure 9.
For the same reaction time 1. EGCG can be seen as the main contributor to DPPH-scavenging activity in green and oolong teas, while ECG was a significant contributor in black and dark teas.
In general, the DPPH-scavenging activity can be mainly attributed to the esterified catechins EGCG or ECG. Based on the results shown in Figure 10 , these minor contributions are in the range of We conducted a systematic study on the total polyphenol and catechins content, as well as antioxidant activity, in four types of tea green, dark, oolong, and black prepared from Camellia sinensis in China.
The highest content of polyphenols and total catechins was detected in green tea, followed by oolong, black, and dark tea.
There was a positive correlation between the antioxidant capacity and total polyphenol content or catechins content ,.
In general, it appears that the longer-fermented teas have lower total polyphenol content, lower catechins content, and lower antioxidant capacity.
According to our results, green tea in China is of very high quality in terms of antioxidant capacity when compared with the other teas.
Results of online HPLC DPPH radical-scavenging activity tests of tea samples showed that gallic acid, EGCG, ECG, EC, EGC, and catechin were responsible for the antioxidant capacity of the extracts from tea samples.
Furthermore, the antioxidant capacity of tea extracts was mainly attributed to the esterified catechins EGCG or ECG.
While consumers will always rely on personal preferences relating to color, taste, and aroma when selecting tea, we believe that the antioxidant capacity should also be considered.
The results of this study should prove useful to any consumers who wish to select tea based on antioxidant capacity.
The authors declare that there is no conflict of interests regarding the publication of this paper. The electrochemical performance of the Bi 2 S 3 samples synthesized in different solvent mixtures was determined using CV and GCD measurements.
The other redox peak pairs observed in Fig. In accordance with the CV results, the GCD discharge curves of the Bi 2 S 3 electrodes Fig.
The relationship between the specific capacitance and current density of the Bi 2 S 3 electrodes determined based on the GCD measurements is shown in Fig.
Specific capacitance vs current density a and Nyquist plots of the tested Bi 2 S 3 electrodes b.
These values are significantly higher than those reported by Nie et al. The resistive properties of the Bi 2 S 3 electrodes were evaluated via EIS analysis Fig.
The impedance spectra consist of a semicircle in the high-frequency region the inset of Fig. These results demonstrate that the Bi 2 S 3 morphology affects the conductive and electrochemical properties of the electrode material.
In turn, the electron propagation mechanism in Bi 2 S 3 micro- and nanospheres is expected to be more random, i.
Ramasamy et al. Distinct variations in the specific capacitance are observed up to the th cycle and are followed by a stabilization period almost a constant capacitance retention in the samples.
This type of behavior has also been reported in previous studies [ 6 , 27 ]. Thus, the improvement in the specific capacitance during cycling could be due to the active surface area for charge storage increasing.
Moreover, morphology rearrangements during cycling can result in the loss of electroactive material, resulting in the gradual capacitance decline [ 26 ].
In conclusion, the solvent system in a solvothermal approach is a critical parameter that determines the morphology of the obtained Bi 2 S 3.
The as-synthesized Bi 2 S 3 samples have different electrochemical behaviors and cycle performances based on their morphologies.
This work encourages the future design and engineering of hybrid materials with a graphene material to further improve the performance of Bi 2 S 3 -based electrodes for supercapacitors.
Yu G, Xie X, Pan L, Bao Z, Cui Y Hybrid nanostructured materials for high-performance electrochemical capacitors. Nano Energy — Ho MY, Khiew PS, Isa D, Tan TK A review of metal oxide composite electrode materials for electrochemical capacitors.
NANO 9 6 — Wiley, London. Google Scholar. Gu W, Yushin G Review of nanostructured carbon materials for electrochemical capacitor applications: advantages and limitations of activated carbon, carbide-derived carbon, zeolite-templated carbon, carbon aerogels, carbon nanotubes, onion-like carbon, and graphene.
WIREs Energy Environ — Toupin M, Brousse T, Belanger D Charge storage mechanism of MnO 2 electrode used in aqueous electrochemical capacitor. Chem Mater 16 16 — Cheng Q, Tang J, Ma J, Zhang H, Shinya N, Qin LCh Graphene and nanostructured MnO 2 composite electrodes for supercapacitors.
Carbon — Electrochim Acta — Energy Technol — On September 15, iKon released the warm-up single "My Type", following lead singles "Rhythm Ta" and "Airplane".
I and fellow member Jinhwan joined the cast of JTBC's Mari and I. I received the Songwriter of the Year award at the 10th Melon Music Awards through iKon's lead single " Love Scenario " from their studio album Return.
I was cast for JTBC 2's variety show Grand Buda-guest in I announced his departure from iKon on June 12, , in a post on his personal Instagram account after news agency Dispatch unearthed KakaoTalk messages from three years prior, outlining his attempt to purchase marijuana and LSD from an undisclosed female dealer.
He was also accused of evading police charges. The messages allegedly detailed a conversation between B. I and the dealer, in which the singer asked for a bulk discount and the dealer warned him about the effects of taking drugs.
I acknowledged the validity of the messages, explaining that he was going "through a hard and painful time" and wanted something to rely on, but denied taking any drugs.
YG Entertainment terminated B. I's contract that same day. I and took drugs together, but was persuaded by the head of his agency Yang Hyun-suk to cover the fact from the police investigation.
P and has received four years of probation in I was released and delivered a negative result. This was after South Korea's Gyeonggi Southern Provincial Police Agency sent a sample of Kim's body hair to the country's National Forensic Service for examination and no illegal drugs were detected.
On September 28, , B. I was appointed as the executive director of the agency IOK Company. As the leader of iKon, B. I was credited with a role in the production and songwriting of all releases under the group, such as their debut full-length studio album, Welcome Back , as well as their singles " WYD" , New Kids: Begin , their second full-length studio album, Return , New Kids: Continue , and New Kids: The Final.
From Wikipedia, the free encyclopedia. South Korean rapper. In this Korean name , the family name is Kim. Skip to main content.
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Madankollu, dik il-presunzjoni hija konfutabbli. Protezzjoni ta' data personali. II The anticipated duration of the interception as known to the issuing authority :.
Skip to main content. This document is an excerpt from the EUR-Lex website.Hampsch-Woodill, and R. About this article. Received 17 May As follows from the XRD patterns in Fig. J Am Chem Soc — Prepare your next career move with Nutroma View vacancy. Spielshows Im Deutschen Fernsehen your next career move with Alaska Yoghurt Drink View vacancy. Ramasamy K, Gupta RK, Sims H, Palchoudhury S, Ivanov S, Gupta A Layered ternary sulfide CuSbS Relax Bilder Lustig nanoplates for flexible solid-state supercapacitors. Piu, F. Toda, S.